基于光谱的SF6分解物中SO2浓度检测仪设计

Design of a spectroscopy-based detector for SO2 concentration in SF6 decomposition products

  • 摘要: 针对电气设备内六氟化硫(SF6)分解物中二氧化硫(SO2)浓度检测问题,对紫外吸收光谱分析模块设计和数据处理方法进行了研究。采用低功耗脉冲氙灯光源缩短预热时间,设计了多次反射的长光程气体吸收池,有效缩短响应时间;光源和微型光谱仪与气室直接耦合,减少用气量,稳定性更好。在280 nm~320 nm谱段进行SO2浓度反演,采用偏最小二乘回归多元校正方法对SO2谱段差分吸光度与SO2浓度建立回归模型,模型误差小于0.5 μL/L。设计了检测仪原理样机,试验验证了设计方案的可行性。

     

    Abstract: Aiming at the detection of SO2 concentration in SF6 decomposition products in electrical equipment, the design of UV absorption spectrum analysis module and data processing method were studied. Low power consumption pulsed xenon lamp light source is used to shorten preheating time. A long optical path gas absorption cell with multiple reflections is designed to effectively shorten the response time. The gas consumption is reduced, and the light source and micro spectrometer are directly coupled with the gas chamber, so that the stability is better. The SO2 concentration was inversed in the 280~320 nm spectral band. The partial least squares regression multiple correction method was used to establish a regression model for the differential absorbance of SO2 spectral band and the SO2 concentration. The errors of the model was less than 0.5 μL/L. The principle prototype is designed, and the feasibility of the design scheme is verified by experiments.

     

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